Three-dimensional structural analysis of polymer/inorganic nanocomposite using FIB-TEMT (focused ion beam - Transmission electron microtomogaraphy)

Noboru Kawase, Mitsuro Kato, Toshiyasu Okui, Hideo Nishioka, Yukihiro Nishikawa, Hiroshi Jinnai

研究成果: Paper査読

抄録

Transmission electron microtomography (TEMT) has been used to study three-dimensional structure of polymer/ZrO 2 nanocomposite. One of the factors that limits the TEMT resolution is the increase of thickness of a microtome section for electron beam transmission when tilted at high-angle. In order to avoid this phenomenon, a rod-shaped sample with a diameter of ca.150nm was fabricated using focused ion beam (FIB) technique. As the result of the FIB-TEMT, high quality 3-D reconstructed image was obtained. In addition, it was confirmed that the rod-shaped fabrication is effective to improve 3-D reconstructed image resolution especially along the thickness direction.

本文言語English
ページ3201-3202
ページ数2
出版ステータスPublished - 2005 12月 1
外部発表はい
イベント54th SPSJ Symposium on Macromolecules - Yamagata, Japan
継続期間: 2005 9月 202005 9月 22

Other

Other54th SPSJ Symposium on Macromolecules
国/地域Japan
CityYamagata
Period05/9/2005/9/22

ASJC Scopus subject areas

  • 工学(全般)

フィンガープリント

「Three-dimensional structural analysis of polymer/inorganic nanocomposite using FIB-TEMT (focused ion beam - Transmission electron microtomogaraphy)」の研究トピックを掘り下げます。これらがまとまってユニークなフィンガープリントを構成します。

引用スタイル