The carbon-boron-titanium compounds were synthesized by hot press and subsequent HIP (high temperature isostatic press) treatment. The thermal diffusivity of the compounds was measured by the advanced laser-flash technique, and the heat-load shock resistance was evaluated with a low energy and high current electron beam. The obtained results were analyzed as a function of chemical composition of the compounds. The so-called gradient material was formed to attempt to improve the heat-load shock resistance.
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