Synthesis and enrichment of titanium subchlorides in molten salts

Osamu Takeda, Toru H. Okabe

研究成果: Conference contribution

2 被引用数 (Scopus)

抄録

With the purpose of establishing a new (semi-)continuous/high-speed titanium production process based on the magnesiothermic reduction of titanium subchlorides (TiClx, x = 2, 3) referred to as the subhalide reduction process, a novel synthetic process for TiClx by using molten salts as the reaction medium was investigated. Titanium tetrachloride (TiCL), supplied by a peristaltic pump at the rate of 0.13-0.72 g/min, was reacted with the feed titanium sponge immersed in molten magnesium chloride (MgCl2) at 1273 K under an argon atmosphere. It was demonstrated that the efficiency of the formation of TiClx was drastically improved by using molten salts as the reaction medium as compared with that of the synthesis by employing the direct reaction of TiCl4 gas with solid titanium. Some results regarding the enrichment of TiClx in molten salts are also shown.

本文言語English
ホスト出版物のタイトルInnovations in Titanium Technology - TMS 2007 Annual Meeting and Exhibition
ページ69-78
ページ数10
出版ステータスPublished - 2007 12 1
イベントInnovations in Titanium Technology - Orlando, FL, United States
継続期間: 2007 2 252007 4 1

出版物シリーズ

名前TMS Annual Meeting

Other

OtherInnovations in Titanium Technology
CountryUnited States
CityOrlando, FL
Period07/2/2507/4/1

ASJC Scopus subject areas

  • Condensed Matter Physics
  • Mechanics of Materials
  • Metals and Alloys

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