Protection-free synthesis of glycosyl dithiocarbamates in aqueous media by using 2-chloroimidazolinium reagent

Gefei Li, Masato Noguchi, Haruka Kashiwagura, Yuuki Tanaka, Kazunari Serizawa, Shin ichiro Shoda

研究成果: Article査読

14 被引用数 (Scopus)

抄録

Glycosyl dithiocarbamates (GDTCs) have been synthesized directly from the corresponding unprotected sugars and dithiocarbamate salts in good yields by using 2-chloro-1,3-dimethylimidazolinium chloride (DMC) as condensing agent in aqueous media. The three-component one-pot synthesis of GDTCs starting from unprotected sugars, carbon disulfide, and secondary amines has also been successfully demonstrated. This is the first report on the direct synthesis of GDTCs from unprotected sugars without using any protecting groups.

本文言語English
ページ(範囲)3529-3531
ページ数3
ジャーナルTetrahedron Letters
57
31
DOI
出版ステータスPublished - 2016

ASJC Scopus subject areas

  • 生化学
  • 創薬
  • 有機化学

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