TY - JOUR
T1 - Microstructure and properties of Ti3SiC2/SiC nanocomposites fabricated by spark plasma sintering
AU - Zhang, Jianfeng
AU - Wu, Ting
AU - Wang, Lianjun
AU - Jiang, Wan
AU - Chen, Lidong
N1 - Funding Information:
This work was supported by the National Science Foundation of China (50625414) and the Open Foundation of State Key Laboratory (No. SKL200504SIC).
PY - 2008/2
Y1 - 2008/2
N2 - High dense Ti3SiC2/SiC nanocomposites with different SiC volume contents were in situ fabricated by spark plasma sintering technique. It is found from microstructural observation that SiC distributes uniformly in the composites. Ti3SiC2 is about 2-10 μm in grain size, but the average grain size of SiC is about 100 nm for the composites containing SiC from 10 to 40 vol%. With the increasing SiC volume contents, Vickers hardness, fracture toughness, thermal conductivity and electrical resistivity of the composites are improved compared to those of monolithic Ti3SiC2. Although the flexural strength of Ti3SiC2/SiC composites decrease slightly, they are higher than reported values, indicating the residual stress caused by thermal expansion mismatch is reduced. The technological implication of this work is that, it not only provides an example for the in situ reactive synthesis of nanocomposites, but also extends the possible application of the novel ternary compound Ti3SiC2 by in situ adding nanosized SiC particles.
AB - High dense Ti3SiC2/SiC nanocomposites with different SiC volume contents were in situ fabricated by spark plasma sintering technique. It is found from microstructural observation that SiC distributes uniformly in the composites. Ti3SiC2 is about 2-10 μm in grain size, but the average grain size of SiC is about 100 nm for the composites containing SiC from 10 to 40 vol%. With the increasing SiC volume contents, Vickers hardness, fracture toughness, thermal conductivity and electrical resistivity of the composites are improved compared to those of monolithic Ti3SiC2. Although the flexural strength of Ti3SiC2/SiC composites decrease slightly, they are higher than reported values, indicating the residual stress caused by thermal expansion mismatch is reduced. The technological implication of this work is that, it not only provides an example for the in situ reactive synthesis of nanocomposites, but also extends the possible application of the novel ternary compound Ti3SiC2 by in situ adding nanosized SiC particles.
KW - A. TiSiC/SiC nanocomposites
KW - B. Spark plasma sintering
KW - C. In situ fabrication
KW - D. Microstructure and properties
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U2 - 10.1016/j.compscitech.2007.06.006
DO - 10.1016/j.compscitech.2007.06.006
M3 - Article
AN - SCOPUS:37349120446
VL - 68
SP - 499
EP - 505
JO - Composites Science and Technology
JF - Composites Science and Technology
SN - 0266-3538
IS - 2
ER -