Mechano-Hydrothermal Synthesis of Tetraborate Pillared Li-Al Layered Double Hydroxides

Jun Qu; Xuewei Li; Zhiwu Lei; Zhao Li; Min Chen; Qiwu Zhang

doi:10.1111/jace.14196

Mechano-Hydrothermal Synthesis of Tetraborate Pillared Li-Al Layered Double Hydroxides

Jun Qu, Xuewei Li, Zhiwu Lei, Zhao Li, Min Chen, Qiwu Zhang

多元物質科学研究所・プロセスシステム工学研究部門

研究成果: Article › 査読

18 被引用数 (Scopus)

抄録

Tetraborate pillared Li-Al layered double hydroxide was synthesized for the first time by a mechano-hydrothermal process in which gibbsite (Al(OH)₃) sample was first activated by a ball milling, followed by hydrothermal treatment with Li₂B₄O₇ in water at 95°C. Activation of gibbsite Al(OH)₃ induced by mechanochemical process was essential for the formation of thin disk-like Li-Al LDH intercalated with borate anion. When in excess the activated Al(OH)₃ was transformed into bayerite phase during the hydrothermal process.

本文言語	English
ページ（範囲）	1151-1154
ページ数	4
ジャーナル	Journal of the American Ceramic Society
巻	99
号	4
DOI	https://doi.org/10.1111/jace.14196
出版ステータス	Published - 2016 4月 1

ASJC Scopus subject areas

セラミックおよび複合材料
材料化学

文献へのアクセス

10.1111/jace.14196

他のファイルとリンク

引用スタイル

@article{62cdaffe20af4e069e54286c7574c609,

title = "Mechano-Hydrothermal Synthesis of Tetraborate Pillared Li-Al Layered Double Hydroxides",

abstract = "Tetraborate pillared Li-Al layered double hydroxide was synthesized for the first time by a mechano-hydrothermal process in which gibbsite (Al(OH)3) sample was first activated by a ball milling, followed by hydrothermal treatment with Li2B4O7 in water at 95°C. Activation of gibbsite Al(OH)3 induced by mechanochemical process was essential for the formation of thin disk-like Li-Al LDH intercalated with borate anion. When in excess the activated Al(OH)3 was transformed into bayerite phase during the hydrothermal process.",

author = "Jun Qu and Xuewei Li and Zhiwu Lei and Zhao Li and Min Chen and Qiwu Zhang",

year = "2016",

month = apr,

day = "1",

doi = "10.1111/jace.14196",

language = "English",

volume = "99",

pages = "1151--1154",

journal = "Journal of the American Ceramic Society",

issn = "0002-7820",

publisher = "Wiley-Blackwell",

number = "4",

}

TY - JOUR

T1 - Mechano-Hydrothermal Synthesis of Tetraborate Pillared Li-Al Layered Double Hydroxides

AU - Qu, Jun

AU - Li, Xuewei

AU - Lei, Zhiwu

AU - Li, Zhao

AU - Chen, Min

AU - Zhang, Qiwu

PY - 2016/4/1

Y1 - 2016/4/1

N2 - Tetraborate pillared Li-Al layered double hydroxide was synthesized for the first time by a mechano-hydrothermal process in which gibbsite (Al(OH)3) sample was first activated by a ball milling, followed by hydrothermal treatment with Li2B4O7 in water at 95°C. Activation of gibbsite Al(OH)3 induced by mechanochemical process was essential for the formation of thin disk-like Li-Al LDH intercalated with borate anion. When in excess the activated Al(OH)3 was transformed into bayerite phase during the hydrothermal process.

AB - Tetraborate pillared Li-Al layered double hydroxide was synthesized for the first time by a mechano-hydrothermal process in which gibbsite (Al(OH)3) sample was first activated by a ball milling, followed by hydrothermal treatment with Li2B4O7 in water at 95°C. Activation of gibbsite Al(OH)3 induced by mechanochemical process was essential for the formation of thin disk-like Li-Al LDH intercalated with borate anion. When in excess the activated Al(OH)3 was transformed into bayerite phase during the hydrothermal process.

UR - http://www.scopus.com/inward/record.url?scp=84960172567&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=84960172567&partnerID=8YFLogxK

U2 - 10.1111/jace.14196

DO - 10.1111/jace.14196

M3 - Article

AN - SCOPUS:84960172567

VL - 99

SP - 1151

EP - 1154

JO - Journal of the American Ceramic Society

JF - Journal of the American Ceramic Society

SN - 0002-7820

IS - 4

ER -

Mechano-Hydrothermal Synthesis of Tetraborate Pillared Li-Al Layered Double Hydroxides

抄録

ASJC Scopus subject areas

文献へのアクセス

他のファイルとリンク

フィンガープリント

引用スタイル