Measurement of hydrated water in D-glucose powder using THz-wave spectroscopy

Kaori Abe, Shin'ichiro Hayashi, Norihito Doki, Chiko Otani, Kodo Kawase, Teruo Miyazawa, Yuichi Ogawa

研究成果: Article査読

9 被引用数 (Scopus)

抄録

In this paper, we introduce a new method to measure the amount of water of crystallization in D-glucose powder using terahertz (THz) wave spectroscopy. We measured five crystalline D-glucose samples: one anhydrous, one monohydrate, and three in various states of partial dehydration, whose water content was measured independently by using Karl Fischer's method. By analyzing the THz absorption spectra, particularly the absorption peaks at 60.3, 65.6, and 80.5 cm -1 , which are strongly correlated with the hydration ratio, we could obtain a highly reliable analytical curve, with a correlation coefficient of 0.9509 and a standard error of prediction of 0.714. This study suggests the possibility of measuring the water of crystallization nondestructively, without using an organic solvent.

本文言語English
ページ(範囲)851-856
ページ数6
ジャーナルBUNSEKI KAGAKU
56
10
DOI
出版ステータスPublished - 2007 12月 17

ASJC Scopus subject areas

  • 分析化学

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