TY - JOUR
T1 - Electrophoretic deposition as a new bioactive glass coating process for orthodontic stainless steel
AU - Kawaguchi, Kyotaro
AU - Iijima, Masahiro
AU - Endo, Kazuhiko
AU - Mizoguchi, Itaru
N1 - Publisher Copyright:
© 2017 by the authors.
PY - 2017/11/1
Y1 - 2017/11/1
N2 - This study investigated the surface modification of orthodontic stainless steel using electrophoretic deposition (EPD) of bioactive glass (BG). The BG coatings were characterized by spectrophotometry, scanning electron microscopy with energy dispersive X-ray spectrometry, and X-ray diffraction. The frictional properties were investigated using a progressive load scratch test. The remineralization ability of the etched dental enamel was studied according to the time-dependent mechanical properties of the enamel using a nano-indentation test. The EPD process using alternating current produced higher values in both reflectance and lightness. Additionally, the BG coating was thinner than that prepared using direct current, and was completely amorphous. All of the BG coatings displayed good interfacial adhesion, and Si and O were the major components. Most BG-coated specimens produced slightly higher frictional forces compared with non-coated specimens. The hardness and elastic modulus of etched enamel specimens immersed with most BG-coated specimens recovered significantly with increasing immersion time compared with the non-coated specimen, and significant acid-neutralization was observed for the BG-coated specimens. The surface modification technique using EPD and BG coating on orthodontic stainless steel may assist the development of new non-cytotoxic orthodontic metallic appliances having satisfactory appearance and remineralization ability.
AB - This study investigated the surface modification of orthodontic stainless steel using electrophoretic deposition (EPD) of bioactive glass (BG). The BG coatings were characterized by spectrophotometry, scanning electron microscopy with energy dispersive X-ray spectrometry, and X-ray diffraction. The frictional properties were investigated using a progressive load scratch test. The remineralization ability of the etched dental enamel was studied according to the time-dependent mechanical properties of the enamel using a nano-indentation test. The EPD process using alternating current produced higher values in both reflectance and lightness. Additionally, the BG coating was thinner than that prepared using direct current, and was completely amorphous. All of the BG coatings displayed good interfacial adhesion, and Si and O were the major components. Most BG-coated specimens produced slightly higher frictional forces compared with non-coated specimens. The hardness and elastic modulus of etched enamel specimens immersed with most BG-coated specimens recovered significantly with increasing immersion time compared with the non-coated specimen, and significant acid-neutralization was observed for the BG-coated specimens. The surface modification technique using EPD and BG coating on orthodontic stainless steel may assist the development of new non-cytotoxic orthodontic metallic appliances having satisfactory appearance and remineralization ability.
KW - Bioactive glass
KW - Electrophoretic deposition
KW - Enamel remineralization
KW - Nanoindentation
KW - Spectrophotometry
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U2 - 10.3390/coatings7110199
DO - 10.3390/coatings7110199
M3 - Article
AN - SCOPUS:85051603643
VL - 7
JO - Coatings
JF - Coatings
SN - 2079-6412
IS - 11
M1 - 199
ER -