TY - JOUR
T1 - Design and testing of Omega mode imaging energy filters at 200 kV
AU - Tsuno, K.
AU - Kaneyama, T.
AU - Honda, T.
AU - Tsuda, K.
AU - Terauchi, M.
AU - Tanaka, M.
PY - 1997
Y1 - 1997
N2 - We designed and constructed an omega filter with following optical properties. The dispersions at 100 and 200 kV are 2.1 and 1.1 μm eV-1, respectively. Non-isochromatisity (difference of the selected energy between the centre and outer regions of an electron microscope image) is 1.3 and 2.5 eV at 100 and 200 kV, respectively, on a 25 mm diameter detector. The filter was installed and tested on a modified 200 kV high resolution TEM with an LaB6 cathode. Zero loss high resolution lattice image of [110]Si in thick specimen regions were clearly observed. Zero loss HOLZ CBED patterns of [111]Si were taken successfully up to 6.4°at an accelerating voltage of 100 kV. Since the slit was inserted to cut 17 eV first plasmon loss of Si, the maximum observable angle limited by the non-isochromatisity is 6.8°, which agrees with the experimental 6.4°. Based on these results, a new omega filter with a non-isochromatisity of 0.9 eV on the diameter 25 mm at 200 kV was designed.
AB - We designed and constructed an omega filter with following optical properties. The dispersions at 100 and 200 kV are 2.1 and 1.1 μm eV-1, respectively. Non-isochromatisity (difference of the selected energy between the centre and outer regions of an electron microscope image) is 1.3 and 2.5 eV at 100 and 200 kV, respectively, on a 25 mm diameter detector. The filter was installed and tested on a modified 200 kV high resolution TEM with an LaB6 cathode. Zero loss high resolution lattice image of [110]Si in thick specimen regions were clearly observed. Zero loss HOLZ CBED patterns of [111]Si were taken successfully up to 6.4°at an accelerating voltage of 100 kV. Since the slit was inserted to cut 17 eV first plasmon loss of Si, the maximum observable angle limited by the non-isochromatisity is 6.8°, which agrees with the experimental 6.4°. Based on these results, a new omega filter with a non-isochromatisity of 0.9 eV on the diameter 25 mm at 200 kV was designed.
KW - Electron energy loss sepectroscopy
KW - Electron optics
KW - Energy analysis
KW - Imaging energy filter
KW - Omega filter
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U2 - 10.1093/oxfordjournals.jmicro.a023531
DO - 10.1093/oxfordjournals.jmicro.a023531
M3 - Article
AN - SCOPUS:0030726615
SN - 2050-5698
VL - 46
SP - 357
EP - 368
JO - Microscopy (Oxford, England)
JF - Microscopy (Oxford, England)
IS - 5
ER -