Control of shell thickness in silica-coating of Agl nanoparticles

Y. Kobayashi, K. Misawa, M. Takeda, N. Ohuchi, A. Kasuya, M. Konno

研究成果: Conference contribution

9 被引用数 (Scopus)

抄録

Silica-coating of AgI nanoparticles with a Stöber method was carried out to find out reaction conditions for control of the shell thickness. The AgI nanoparticles were prepared from AgC1O4 and KI with the use of 3-mercaptopropyltrimethoxysilane (MPS) as a silane coupling agent and dimethylamine (DMA) catalyst for alkoxide hydrolysis. The silica-coating was performed at 4.5×10-6-4.5×10-5 M MPS, 11-20 M water, 0.002-0.1 M DMA and 0.005-0.04 M tetraethylorthosilicate at AgI concentrations of 0.1-1 mM. Consequently, AgI-silica core-shell particles could be prepared with the use of 4.5×10-5 M MPS, 20 M water, 0.01 M DMA and 1 mM AgI. Silica shell thickness could be varied from 15 to 28 nm with an increase in the TEOS concentration from 0.005 to 0.04 M.

本文言語English
ホスト出版物のタイトルAdvanced Materials and Processing IV - Selected, peer reviewed papers presented at the 4th International Conference on Advanced Materials and Processing
出版社Trans Tech Publications
ページ191-194
ページ数4
ISBN(印刷版)0878494669, 9780878494668
DOI
出版ステータスPublished - 2007
イベント4th International Conference on Advanced Materials and Processing, ICAMP-4 - Hamilton, New Zealand
継続期間: 2006 12月 102006 12月 13

出版物シリーズ

名前Advanced Materials Research
29-30
ISSN(印刷版)1022-6680

Other

Other4th International Conference on Advanced Materials and Processing, ICAMP-4
国/地域New Zealand
CityHamilton
Period06/12/1006/12/13

ASJC Scopus subject areas

  • 工学(全般)

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