Abstract
The effect of post-sintering heat treatment on the coercivity of Nd-Fe-B based permanent magnets was studied by observing their crystallographic and magnetic microstructures. High-resolution transmission electron microscopy revealed meandering grain boundaries in die as-sintered state, and the smoothness of the boundaries was improved by the post-sintering heat treatment. Electron holography demonstrated that magnetization reversal occurred in a stepwise manner in individual grains in the specimen subjected to the post-sintering heat treatment, whereas reversal was occurred simultaneously in different grains in the as-sintered specimen.
| Original language | English |
|---|---|
| Pages (from-to) | 333-340 |
| Number of pages | 8 |
| Journal | Materials Transactions |
| Volume | 51 |
| Issue number | 2 |
| DOIs | |
| Publication status | Published - 2010 Feb 1 |
Keywords
- Coercivity
- Domain wall
- Electron holography
- Lorentz microscopy
- Permanent magnet
ASJC Scopus subject areas
- Materials Science(all)
- Condensed Matter Physics
- Mechanics of Materials
- Mechanical Engineering
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Sato, K., Murakami, Y., Shindo, D., Hirosawa, S., & Yasuhara, A. (2010). Transmission electron microscopy study on the grain boundaries and magnetic domains in Nd-Fe-B based magnets. Materials Transactions, 51(2), 333-340. https://doi.org/10.2320/matertrans.M2009277