Trace analysis of released metallic ions in static immersion test for characterization of metallic biomaterials

Tetsuya Asnino; Naofumi Ohtsu; Kazuaki Wagatsuma

doi:10.2320/matertrans.MRA2007325

Trace analysis of released metallic ions in static immersion test for characterization of metallic biomaterials

Tetsuya Asnino, Naofumi Ohtsu, Kazuaki Wagatsuma

Materials Processing and Characterization Division

Research output: Contribution to journal › Article › peer-review

4 Citations (Scopus)

Abstract

For characterization of corrosion resistance of metallic biomaterials, determination of trace amounts of metallic ions released from the materials in using static immersion into simulated body fluids (SBF) were investigated. In using a H₂SO₄-fume pre-treatment method, sensitive, precise and accurate determination of the trace metallic elements in SBFs could be performed by ICP-OES. For accurate analysis, it was necessary to employ a matrix-matched solution for the calibration. Moreover, usage of a PFA vessel in the static immersion test was recommended for the prevention of contamination. Thus, it was possible to determine μg dm^-3 (ppb) order of elements in SBFs and evaluate nano-gram order of the released metallic ions.

Original language	English
Pages (from-to)	1342-1345
Number of pages	4
Journal	Materials Transactions
Volume	49
Issue number	6
DOIs	https://doi.org/10.2320/matertrans.MRA2007325
Publication status	Published - 2008 Jun

Keywords

Inductively coupled plasma-optical emission spectrometry
Metallic biomaterials
Simulated body fluid
Static immersion test

ASJC Scopus subject areas

Materials Science(all)
Condensed Matter Physics
Mechanics of Materials
Mechanical Engineering

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10.2320/matertrans.MRA2007325

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title = "Trace analysis of released metallic ions in static immersion test for characterization of metallic biomaterials",

abstract = "For characterization of corrosion resistance of metallic biomaterials, determination of trace amounts of metallic ions released from the materials in using static immersion into simulated body fluids (SBF) were investigated. In using a H2SO4-fume pre-treatment method, sensitive, precise and accurate determination of the trace metallic elements in SBFs could be performed by ICP-OES. For accurate analysis, it was necessary to employ a matrix-matched solution for the calibration. Moreover, usage of a PFA vessel in the static immersion test was recommended for the prevention of contamination. Thus, it was possible to determine μg dm-3 (ppb) order of elements in SBFs and evaluate nano-gram order of the released metallic ions.",

keywords = "Inductively coupled plasma-optical emission spectrometry, Metallic biomaterials, Simulated body fluid, Static immersion test",

author = "Tetsuya Asnino and Naofumi Ohtsu and Kazuaki Wagatsuma",

year = "2008",

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language = "English",

volume = "49",

pages = "1342--1345",

journal = "Materials Transactions",

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T1 - Trace analysis of released metallic ions in static immersion test for characterization of metallic biomaterials

AU - Asnino, Tetsuya

AU - Ohtsu, Naofumi

AU - Wagatsuma, Kazuaki

PY - 2008/6

Y1 - 2008/6

N2 - For characterization of corrosion resistance of metallic biomaterials, determination of trace amounts of metallic ions released from the materials in using static immersion into simulated body fluids (SBF) were investigated. In using a H2SO4-fume pre-treatment method, sensitive, precise and accurate determination of the trace metallic elements in SBFs could be performed by ICP-OES. For accurate analysis, it was necessary to employ a matrix-matched solution for the calibration. Moreover, usage of a PFA vessel in the static immersion test was recommended for the prevention of contamination. Thus, it was possible to determine μg dm-3 (ppb) order of elements in SBFs and evaluate nano-gram order of the released metallic ions.

AB - For characterization of corrosion resistance of metallic biomaterials, determination of trace amounts of metallic ions released from the materials in using static immersion into simulated body fluids (SBF) were investigated. In using a H2SO4-fume pre-treatment method, sensitive, precise and accurate determination of the trace metallic elements in SBFs could be performed by ICP-OES. For accurate analysis, it was necessary to employ a matrix-matched solution for the calibration. Moreover, usage of a PFA vessel in the static immersion test was recommended for the prevention of contamination. Thus, it was possible to determine μg dm-3 (ppb) order of elements in SBFs and evaluate nano-gram order of the released metallic ions.

KW - Inductively coupled plasma-optical emission spectrometry

KW - Metallic biomaterials

KW - Simulated body fluid

KW - Static immersion test

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Trace analysis of released metallic ions in static immersion test for characterization of metallic biomaterials

Abstract

Keywords

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