Three-dimensional structural analysis of multi-component nano-fillers in rubbery matrix studied by transmission electron microtomography

Yuki Shinbori; Hidekazu Sugimori; Yukihiro Nishikawa; Hiroshi Jinnai; Keizo Akutagawa; Naruhiko Mashita; Toshio Nishi

Three-dimensional structural analysis of multi-component nano-fillers in rubbery matrix studied by transmission electron microtomography

Yuki Shinbori, Hidekazu Sugimori, Yukihiro Nishikawa, Hiroshi Jinnai, Keizo Akutagawa, Naruhiko Mashita, Toshio Nishi

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution

Abstract

Three-dimensional (3D) structure of rubber containing two kinds of nano-filler, i.e., carbon black (CB) and silica (Si) particles, has been studied by transmission electron microtomography (TEMT) together with electron energy loss spectroscopy (EELS). Some structural parameters, e.g. particle size and their distributions, were evaluated independently for the CB and Si particles from the 3D reconstruction of the TEMT. In addition, spherical particles were packed into the region of aggregates of the TEMT image using Monte Carlo type simulation. Details of 3D quantitative image analysis as well as the experimental technique will be discussed at the conference time.

Original language	English
Title of host publication	Polymer Preprints, Japan
Pages	994
Number of pages	1
Volume	55
Edition	1
Publication status	Published - 2006
Externally published	Yes
Event	55th SPSJ Annual Meeting - Nagoya, Japan Duration: 2006 May 24 → 2006 May 26

Other

Other	55th SPSJ Annual Meeting
Country/Territory	Japan
City	Nagoya
Period	06/5/24 → 06/5/26

Keywords

Electron energy loss spectroscopy
Filler distribution
Three dimensional observation
Transmission Electron Microtomography

ASJC Scopus subject areas

Engineering(all)

Cite this

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title = "Three-dimensional structural analysis of multi-component nano-fillers in rubbery matrix studied by transmission electron microtomography",

abstract = "Three-dimensional (3D) structure of rubber containing two kinds of nano-filler, i.e., carbon black (CB) and silica (Si) particles, has been studied by transmission electron microtomography (TEMT) together with electron energy loss spectroscopy (EELS). Some structural parameters, e.g. particle size and their distributions, were evaluated independently for the CB and Si particles from the 3D reconstruction of the TEMT. In addition, spherical particles were packed into the region of aggregates of the TEMT image using Monte Carlo type simulation. Details of 3D quantitative image analysis as well as the experimental technique will be discussed at the conference time.",

keywords = "Electron energy loss spectroscopy, Filler distribution, Three dimensional observation, Transmission Electron Microtomography",

author = "Yuki Shinbori and Hidekazu Sugimori and Yukihiro Nishikawa and Hiroshi Jinnai and Keizo Akutagawa and Naruhiko Mashita and Toshio Nishi",

year = "2006",

language = "English",

volume = "55",

pages = "994",

booktitle = "Polymer Preprints, Japan",

edition = "1",

note = "55th SPSJ Annual Meeting ; Conference date: 24-05-2006 Through 26-05-2006",

}

TY - GEN

T1 - Three-dimensional structural analysis of multi-component nano-fillers in rubbery matrix studied by transmission electron microtomography

AU - Shinbori, Yuki

AU - Sugimori, Hidekazu

AU - Nishikawa, Yukihiro

AU - Jinnai, Hiroshi

AU - Akutagawa, Keizo

AU - Mashita, Naruhiko

AU - Nishi, Toshio

PY - 2006

Y1 - 2006

N2 - Three-dimensional (3D) structure of rubber containing two kinds of nano-filler, i.e., carbon black (CB) and silica (Si) particles, has been studied by transmission electron microtomography (TEMT) together with electron energy loss spectroscopy (EELS). Some structural parameters, e.g. particle size and their distributions, were evaluated independently for the CB and Si particles from the 3D reconstruction of the TEMT. In addition, spherical particles were packed into the region of aggregates of the TEMT image using Monte Carlo type simulation. Details of 3D quantitative image analysis as well as the experimental technique will be discussed at the conference time.

AB - Three-dimensional (3D) structure of rubber containing two kinds of nano-filler, i.e., carbon black (CB) and silica (Si) particles, has been studied by transmission electron microtomography (TEMT) together with electron energy loss spectroscopy (EELS). Some structural parameters, e.g. particle size and their distributions, were evaluated independently for the CB and Si particles from the 3D reconstruction of the TEMT. In addition, spherical particles were packed into the region of aggregates of the TEMT image using Monte Carlo type simulation. Details of 3D quantitative image analysis as well as the experimental technique will be discussed at the conference time.

KW - Electron energy loss spectroscopy

KW - Filler distribution

KW - Three dimensional observation

KW - Transmission Electron Microtomography

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M3 - Conference contribution

AN - SCOPUS:33749659894

VL - 55

SP - 994

BT - Polymer Preprints, Japan

T2 - 55th SPSJ Annual Meeting

Y2 - 24 May 2006 through 26 May 2006

ER -

Three-dimensional structural analysis of multi-component nano-fillers in rubbery matrix studied by transmission electron microtomography

Abstract

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Keywords

ASJC Scopus subject areas

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