Synthesis of Li 1+x V 3O 8 by chemical route and its characterization

Selvasekarapandian Subramanian, Sakunthala Ayyasamy, P. Christopher Selvin, M. V. Reddy, B. V.R. Chowdari, Nithya Heller, Arunkumar Dorai, Hema Muthusamy

Research output: Contribution to journalArticlepeer-review

2 Citations (Scopus)

Abstract

Lithium trivanadate (Li 1+xV 3O 8) nanorods have been synthesized by the simple polymer precursor route using the polymer, polyvinyl pyrrolidone (PVP) as the complexing agent. Thermal behavior of the precursor has been studied by the differential scanning calorimetry (DSC), thermogravimetric analysis (TGA) and differential thermal analysis (DTA) techniques. X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FTIR) studies confirm the formation of the compound. High resolution scanning electron microscopy (HRSEM) analysis reveals the synthesized Li 1.2V 3O 8 particles to be nanorods with an average diameter of 50 nm.

Original languageEnglish
Pages (from-to)737-742
Number of pages6
JournalJournal of Nanoscience and Nanotechnology
Volume12
Issue number1
DOIs
Publication statusPublished - 2012
Externally publishedYes

Keywords

  • Cathode material
  • Conductivity
  • Li V O
  • Nanorods
  • PVP

ASJC Scopus subject areas

  • Bioengineering
  • Chemistry(all)
  • Biomedical Engineering
  • Materials Science(all)
  • Condensed Matter Physics

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