The palladium-catalyzed reaction of 4,6-diiodo-2-methylpyrimidine with 5-trimethylsilylpent-4-yn-1-ylzinc iodide gave 4,6-bis(5-trimethylsilylpent-4-yn-1-yl)-2-methyl-pyrimidine. Desilylation of the product followed by treatment with cupric acetate gave 13-methyl(4,6)pyrimidinophane.
|Number of pages||4|
|Publication status||Published - 1988 Feb 1|
ASJC Scopus subject areas
- Analytical Chemistry
- Organic Chemistry