TY - JOUR
T1 - Synthesis and characterization of bulky FSM with interconnected mesopore-networks using an HHP method
AU - Takimura, Mari
AU - Nagata, Hidezumi
AU - Yamasaki, Yuki
AU - Suzuki, Toshiyuki
AU - Ikuhara, Yuichi
AU - Nakahira, Atsushi
N1 - Copyright:
Copyright 2017 Elsevier B.V., All rights reserved.
PY - 2006/6
Y1 - 2006/6
N2 - In this study, the synthesis of bulky FSM materials was attempted by a hydrothermal hot-pressing (HHP) method at relatively low temperatures. The obtained FSM bulks had dense microstructures without large voids and extremely high values of specific surface areas of over 1000 m2/g. TEM observations showed that the bulks synthesized by this HHP method possessed a regular hexagonal arrangement of uniform mesopores and no amorphous phase at the interface between FSM grains, leading to bulky FSM bodies with interconnected mesopore-networks. As a result, dense bulky bodies with hexagonal structured mesopores and high values of specific surface areas could be obtained by this HHP method. These bulky FSM bodies are expected to be applicable as catalysts, adsorbents, sensors, electronics materials, and so on.
AB - In this study, the synthesis of bulky FSM materials was attempted by a hydrothermal hot-pressing (HHP) method at relatively low temperatures. The obtained FSM bulks had dense microstructures without large voids and extremely high values of specific surface areas of over 1000 m2/g. TEM observations showed that the bulks synthesized by this HHP method possessed a regular hexagonal arrangement of uniform mesopores and no amorphous phase at the interface between FSM grains, leading to bulky FSM bodies with interconnected mesopore-networks. As a result, dense bulky bodies with hexagonal structured mesopores and high values of specific surface areas could be obtained by this HHP method. These bulky FSM bodies are expected to be applicable as catalysts, adsorbents, sensors, electronics materials, and so on.
KW - Dense microstructure
KW - FSM
KW - HHP
KW - Hydrothermal hot-pressing
KW - Interconnected mesopore-networks
KW - Mesoporous silica
UR - http://www.scopus.com/inward/record.url?scp=33744900331&partnerID=8YFLogxK
UR - http://www.scopus.com/inward/citedby.url?scp=33744900331&partnerID=8YFLogxK
U2 - 10.2109/jcersj.114.554
DO - 10.2109/jcersj.114.554
M3 - Article
AN - SCOPUS:33744900331
VL - 114
SP - 554
EP - 557
JO - Nippon Seramikkusu Kyokai Gakujutsu Ronbunshi/Journal of the Ceramic Society of Japan
JF - Nippon Seramikkusu Kyokai Gakujutsu Ronbunshi/Journal of the Ceramic Society of Japan
SN - 1882-0743
IS - 1330
ER -