Small-Angle X-ray Scattering of Heat-Treated Flame-Fused Silica Glass from Amorphous and Crystalline Powders

A. H. Shinohara; K. Omote; E. H. Sekiya; K. Shinoda; D. Torikai; C. K. Suzuki; C. A.C. Zavaglia

doi:10.1107/S0021889897003130

Small-Angle X-ray Scattering of Heat-Treated Flame-Fused Silica Glass from Amorphous and Crystalline Powders

A. H. Shinohara, K. Omote, E. H. Sekiya, K. Shinoda, D. Torikai, C. K. Suzuki, C. A.C. Zavaglia

Division of Inorganic Material Research

Research output: Contribution to journal › Article › peer-review

Abstract

High-quality as-fused silica glass, heat treated at 1523 K and prepared by the flame-fusion process using natural crystalline quartz and high-purity amorphous silica glass powders, was investigated by small-angle X-ray scattering (SAXS). The X-ray scattering intensity amplitude from the amorphous structure after heat treatment was analysed in terms of viscosity, density and metallic impurity content. It is shown that SAXS scattering of the amorphous sample is sensitive to the structural change induced by annealing.

Original language	English
Pages (from-to)	918-920
Number of pages	3
Journal	Journal of Applied Crystallography
Volume	30
Issue number	6
DOIs	https://doi.org/10.1107/S0021889897003130
Publication status	Published - 1997 Dec 1

ASJC Scopus subject areas

Biochemistry, Genetics and Molecular Biology(all)

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title = "Small-Angle X-ray Scattering of Heat-Treated Flame-Fused Silica Glass from Amorphous and Crystalline Powders",

abstract = "High-quality as-fused silica glass, heat treated at 1523 K and prepared by the flame-fusion process using natural crystalline quartz and high-purity amorphous silica glass powders, was investigated by small-angle X-ray scattering (SAXS). The X-ray scattering intensity amplitude from the amorphous structure after heat treatment was analysed in terms of viscosity, density and metallic impurity content. It is shown that SAXS scattering of the amorphous sample is sensitive to the structural change induced by annealing.",

author = "Shinohara, {A. H.} and K. Omote and Sekiya, {E. H.} and K. Shinoda and D. Torikai and Suzuki, {C. K.} and Zavaglia, {C. A.C.}",

year = "1997",

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AU - Shinohara, A. H.

AU - Omote, K.

AU - Sekiya, E. H.

AU - Shinoda, K.

AU - Torikai, D.

AU - Suzuki, C. K.

AU - Zavaglia, C. A.C.

PY - 1997/12/1

Y1 - 1997/12/1

N2 - High-quality as-fused silica glass, heat treated at 1523 K and prepared by the flame-fusion process using natural crystalline quartz and high-purity amorphous silica glass powders, was investigated by small-angle X-ray scattering (SAXS). The X-ray scattering intensity amplitude from the amorphous structure after heat treatment was analysed in terms of viscosity, density and metallic impurity content. It is shown that SAXS scattering of the amorphous sample is sensitive to the structural change induced by annealing.

AB - High-quality as-fused silica glass, heat treated at 1523 K and prepared by the flame-fusion process using natural crystalline quartz and high-purity amorphous silica glass powders, was investigated by small-angle X-ray scattering (SAXS). The X-ray scattering intensity amplitude from the amorphous structure after heat treatment was analysed in terms of viscosity, density and metallic impurity content. It is shown that SAXS scattering of the amorphous sample is sensitive to the structural change induced by annealing.

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Small-Angle X-ray Scattering of Heat-Treated Flame-Fused Silica Glass from Amorphous and Crystalline Powders

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