Six-axis multi-anvil press for high-pressure, high-temperature neutron diffraction experiments

A. Sano-Furukawa, T. Hattori, H. Arima, A. Yamada, S. Tabata, M. Kondo, A. Nakamura, H. Kagi, T. Yagi

Research output: Contribution to journalArticlepeer-review

36 Citations (Scopus)

Abstract

We developed a six-axis multi-anvil press, ATSUHIME, for high-pressure and high-temperature in situ time-of-flight neutron powder diffraction experiments. The press has six orthogonally oriented hydraulic rams that operate individually to compress a cubic sample assembly. Experiments indicate that the press can generate pressures up to 9.3 GPa and temperatures up to 2000 K using a 6-6-type cell assembly, with available sample volume of about 50 mm3. Using a 6-8-type cell assembly, the available conditions expand to 16 GPa and 1273 K. Because the six-axis press has no guide blocks, there is sufficient space around the sample to use the aperture for diffraction and place an incident slit, radial collimators, and a neutron imaging camera close to the sample. Combination of the sixaxis press and the collimation devices realized high-quality diffraction pattern with no contamination from the heater or the sample container surrounding the sample. This press constitutes a new tool for using neutron diffraction to study the structures of crystals and liquids under high pressures and temperatures.

Original languageEnglish
Article number113905
JournalReview of Scientific Instruments
Volume85
Issue number11
DOIs
Publication statusPublished - 2014 Nov 1

ASJC Scopus subject areas

  • Instrumentation

Fingerprint

Dive into the research topics of 'Six-axis multi-anvil press for high-pressure, high-temperature neutron diffraction experiments'. Together they form a unique fingerprint.

Cite this