Separation of carrier free 95mTc from niobium targets irradiated with alpha-particles

T. Sekine; M. Konishi; H. Kudo; K. Tagami; S. Uchida

doi:10.1007/BF02349055

Separation of carrier free ^95mTc from niobium targets irradiated with alpha-particles

T. Sekine, M. Konishi, H. Kudo, K. Tagami, S. Uchida

Division of Developmental Research in Education Programs

Research output: Contribution to journal › Article › peer-review

13 Citations (Scopus)

Abstract

A ^95mTc tracer with an excellent quality was prepared by a simple sublimation method after α-bombardment of niobium metal. Technetium-95m produced by the ⁹³Nb(α,2n)^95mTc reaction was separated from the niobium targets in a quartz tube by heating at 1100 °C in an oxygen gas flow. Technetium-95m sublimed as an oxide was deposited on the inner wall of the quartz tube outside an electric furnace, and then collected as a pertechnetate solution by washing with water. The ICP-MS analysis of the ^95mTc solution revealed its excellent quality, compared to a ^95mTc solution prepared from the same targets through a wet chemical separation method and a commercial ^95mTc solution. With this tracer, the precision of ICP-MS analysis of ⁹⁹Tc in environmental samples are highly improved.

Original language	English
Pages (from-to)	483-487
Number of pages	5
Journal	Journal of Radioanalytical and Nuclear Chemistry
Volume	239
Issue number	3
DOIs	https://doi.org/10.1007/BF02349055
Publication status	Published - 1999 Jan 1

ASJC Scopus subject areas

Analytical Chemistry
Nuclear Energy and Engineering
Radiology Nuclear Medicine and imaging
Pollution
Spectroscopy
Public Health, Environmental and Occupational Health
Health, Toxicology and Mutagenesis

UN SDGs

This output contributes to the following Sustainable Development Goal(s)

Access to Document

10.1007/BF02349055

Fingerprint Dive into the research topics of 'Separation of carrier free <sup>95m</sup>Tc from niobium targets irradiated with alpha-particles'. Together they form a unique fingerprint.

Cite this

@article{ccbf31f184c246b3a8f408d436e89912,

title = "Separation of carrier free 95mTc from niobium targets irradiated with alpha-particles",

abstract = "A 95mTc tracer with an excellent quality was prepared by a simple sublimation method after α-bombardment of niobium metal. Technetium-95m produced by the 93Nb(α,2n)95mTc reaction was separated from the niobium targets in a quartz tube by heating at 1100 °C in an oxygen gas flow. Technetium-95m sublimed as an oxide was deposited on the inner wall of the quartz tube outside an electric furnace, and then collected as a pertechnetate solution by washing with water. The ICP-MS analysis of the 95mTc solution revealed its excellent quality, compared to a 95mTc solution prepared from the same targets through a wet chemical separation method and a commercial 95mTc solution. With this tracer, the precision of ICP-MS analysis of 99Tc in environmental samples are highly improved.",

author = "T. Sekine and M. Konishi and H. Kudo and K. Tagami and S. Uchida",

year = "1999",

month = jan,

day = "1",

doi = "10.1007/BF02349055",

language = "English",

volume = "239",

pages = "483--487",

journal = "Journal of Radioanalytical and Nuclear Chemistry",

issn = "0022-4081",

publisher = "Elsevier BV",

number = "3",

}

TY - JOUR

T1 - Separation of carrier free 95mTc from niobium targets irradiated with alpha-particles

AU - Sekine, T.

AU - Konishi, M.

AU - Kudo, H.

AU - Tagami, K.

AU - Uchida, S.

PY - 1999/1/1

Y1 - 1999/1/1

N2 - A 95mTc tracer with an excellent quality was prepared by a simple sublimation method after α-bombardment of niobium metal. Technetium-95m produced by the 93Nb(α,2n)95mTc reaction was separated from the niobium targets in a quartz tube by heating at 1100 °C in an oxygen gas flow. Technetium-95m sublimed as an oxide was deposited on the inner wall of the quartz tube outside an electric furnace, and then collected as a pertechnetate solution by washing with water. The ICP-MS analysis of the 95mTc solution revealed its excellent quality, compared to a 95mTc solution prepared from the same targets through a wet chemical separation method and a commercial 95mTc solution. With this tracer, the precision of ICP-MS analysis of 99Tc in environmental samples are highly improved.

AB - A 95mTc tracer with an excellent quality was prepared by a simple sublimation method after α-bombardment of niobium metal. Technetium-95m produced by the 93Nb(α,2n)95mTc reaction was separated from the niobium targets in a quartz tube by heating at 1100 °C in an oxygen gas flow. Technetium-95m sublimed as an oxide was deposited on the inner wall of the quartz tube outside an electric furnace, and then collected as a pertechnetate solution by washing with water. The ICP-MS analysis of the 95mTc solution revealed its excellent quality, compared to a 95mTc solution prepared from the same targets through a wet chemical separation method and a commercial 95mTc solution. With this tracer, the precision of ICP-MS analysis of 99Tc in environmental samples are highly improved.

UR - http://www.scopus.com/inward/record.url?scp=0032924082&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=0032924082&partnerID=8YFLogxK

U2 - 10.1007/BF02349055

DO - 10.1007/BF02349055

M3 - Article

AN - SCOPUS:0032924082

VL - 239

SP - 483

EP - 487

JO - Journal of Radioanalytical and Nuclear Chemistry

JF - Journal of Radioanalytical and Nuclear Chemistry

SN - 0022-4081

IS - 3

ER -