Self-assembly of the mesoporous electrode material Li3Fe 2(PO4)3 using a cationic surfactant as the template

Shenmin Zhu; Haoshen Zhou; Toshikazu Miyoshi; Mitsuhiro Hibino; Itaru Honma; Masaki Ichihara

doi:10.1002/adma.200400207

Self-assembly of the mesoporous electrode material Li₃Fe ₂(PO₄)₃ using a cationic surfactant as the template

Shenmin Zhu, Haoshen Zhou, Toshikazu Miyoshi, Mitsuhiro Hibino, Itaru Honma, Masaki Ichihara

Research output: Contribution to journal › Article › peer-review

60 Citations (Scopus)

Abstract

The self assembly of mesoporous multi-metal phosphates was analyzed by using a cationic surfactant as the template. Two distinct diffraction peaks were observed from the powder X-ray diffraction patterns before and after calcination. It was also observed that the greatest loss of weight occurred at 230°C, while no weight loss was detected for the calcined sample between the temperatures of 150 and 500°C. It was found that the disappearance of the C-H valency bond vibrations at about 2844 cm^-1 and 2920 cm ^-1 in the calcined material confirmed the complete removal of the surfactant at 623K.

Original language	English
Pages (from-to)	2012-2017
Number of pages	6
Journal	Advanced Materials
Volume	16
Issue number	22
DOIs	https://doi.org/10.1002/adma.200400207
Publication status	Published - 2004 Nov 18
Externally published	Yes

ASJC Scopus subject areas

Materials Science(all)
Mechanics of Materials
Mechanical Engineering

Access to Document

10.1002/adma.200400207

Cite this

@article{0a9b832e1cbb4cc9bad286740e9f128f,

title = "Self-assembly of the mesoporous electrode material Li3Fe 2(PO4)3 using a cationic surfactant as the template",

abstract = "The self assembly of mesoporous multi-metal phosphates was analyzed by using a cationic surfactant as the template. Two distinct diffraction peaks were observed from the powder X-ray diffraction patterns before and after calcination. It was also observed that the greatest loss of weight occurred at 230°C, while no weight loss was detected for the calcined sample between the temperatures of 150 and 500°C. It was found that the disappearance of the C-H valency bond vibrations at about 2844 cm-1 and 2920 cm -1 in the calcined material confirmed the complete removal of the surfactant at 623K.",

author = "Shenmin Zhu and Haoshen Zhou and Toshikazu Miyoshi and Mitsuhiro Hibino and Itaru Honma and Masaki Ichihara",

year = "2004",

month = nov,

day = "18",

doi = "10.1002/adma.200400207",

language = "English",

volume = "16",

pages = "2012--2017",

journal = "Advanced Materials",

issn = "0935-9648",

publisher = "Wiley-VCH Verlag",

number = "22",

}

TY - JOUR

T1 - Self-assembly of the mesoporous electrode material Li3Fe 2(PO4)3 using a cationic surfactant as the template

AU - Zhu, Shenmin

AU - Zhou, Haoshen

AU - Miyoshi, Toshikazu

AU - Hibino, Mitsuhiro

AU - Honma, Itaru

AU - Ichihara, Masaki

PY - 2004/11/18

Y1 - 2004/11/18

N2 - The self assembly of mesoporous multi-metal phosphates was analyzed by using a cationic surfactant as the template. Two distinct diffraction peaks were observed from the powder X-ray diffraction patterns before and after calcination. It was also observed that the greatest loss of weight occurred at 230°C, while no weight loss was detected for the calcined sample between the temperatures of 150 and 500°C. It was found that the disappearance of the C-H valency bond vibrations at about 2844 cm-1 and 2920 cm -1 in the calcined material confirmed the complete removal of the surfactant at 623K.

AB - The self assembly of mesoporous multi-metal phosphates was analyzed by using a cationic surfactant as the template. Two distinct diffraction peaks were observed from the powder X-ray diffraction patterns before and after calcination. It was also observed that the greatest loss of weight occurred at 230°C, while no weight loss was detected for the calcined sample between the temperatures of 150 and 500°C. It was found that the disappearance of the C-H valency bond vibrations at about 2844 cm-1 and 2920 cm -1 in the calcined material confirmed the complete removal of the surfactant at 623K.

UR - http://www.scopus.com/inward/record.url?scp=11444250544&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=11444250544&partnerID=8YFLogxK

U2 - 10.1002/adma.200400207

DO - 10.1002/adma.200400207

M3 - Article

AN - SCOPUS:11444250544

VL - 16

SP - 2012

EP - 2017

JO - Advanced Materials

JF - Advanced Materials

SN - 0935-9648

IS - 22

ER -

Self-assembly of the mesoporous electrode material Li₃Fe ₂(PO₄)₃ using a cationic surfactant as the template

Abstract

ASJC Scopus subject areas

Access to Document

Other files and links

Fingerprint

Cite this