Quantifying Nanosheet Graphene Oxide Using Electrospray-Differential Mobility Analysis

Jui Ting Tai, Yen Chih Lai, Jian He Yang, Hsin Chia Ho, Hsiao Fang Wang, Rong Ming Ho, De Hao Tsai

Research output: Contribution to journalArticlepeer-review

19 Citations (Scopus)

Abstract

(Graph Presented) We report a high-resolution, traceable method to quantify number concentrations and dimensional properties of nanosheet graphene oxide (N-GO) colloids using electrospray-differential mobility analysis (ES-DMA). Transmission electron microscopy (TEM) was employed orthogonally to provide complementary data and imagery of N-GOs. Results show that the equivalent mobility sizes, size distributions, and number concentrations of N-GOs were able to be successfully measured by ES-DMA. Colloidal stability and filtration efficiency of N-GOs were shown to be effectively characterized based on the change of size distributions and number concentrations. Through the use of an analytical model, the DMA data were able to be converted into lateral size distributions, showing the average lateral size of N-GOs was ∼32 nm with an estimated thickness ∼0.8 nm. This prototype study demonstrates the proof of concept of using ES-DMA to quantitatively characterize N-GOs and provides traceability for applications involving the formulation of N-GOs.

Original languageEnglish
Pages (from-to)3884-3889
Number of pages6
JournalAnalytical Chemistry
Volume87
Issue number7
DOIs
Publication statusPublished - 2015 Apr 7
Externally publishedYes

ASJC Scopus subject areas

  • Analytical Chemistry

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