Protection-free synthesis of alkyl glycosides under hydrogenolytic conditions

Masaki Ishihara, Yuka Takagi, Gefei Li, Masato Noguchi, Shinichiro Shoda

Research output: Contribution to journalArticlepeer-review

4 Citations (Scopus)

Abstract

A convenient protection-free synthetic route for the preparation of alkyl glycosides has been developed. The alcoholysis of one-step preparable glycosyl donors, 4,6-dibenzyloxy-1,3,5-triazin-2-yl (DBT) glycosides, under hydrogenolytic conditions gave the corresponding glycosides in good yields without the addition of any acid promoters. The method could be successfully applied to the glycosylation of an acidlabile oligosaccharide.

Original languageEnglish
Pages (from-to)1235-1237
Number of pages3
JournalChemistry Letters
Volume42
Issue number10
DOIs
Publication statusPublished - 2013 Oct 16

ASJC Scopus subject areas

  • Chemistry(all)

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