Preparation of multideuterated 5-deoxystrigol for use as an internal standard for quantitative LC/MS

Kotomi Ueno, Atsushi Hanada, Shinjiro Yamaguchi, Tadao Asami

    Research output: Contribution to journalArticlepeer-review

    13 Citations (Scopus)

    Abstract

    We prepared deuterium-labeled 5-deoxystrigol (5DS), a multifunctional plant second metabolite, using a simple set of procedures. The labeled compound contained mainly [3a,4,4,5,5,6′-D6]-5DS and [D5]-5DS and did not contain unlabeled 5DS. Therefore, multideuterated 5DS can be used as an internal standard in liquid chromatography/mass spectrometry (LC/MS) assays to quantitate the amounts of 5DS in plants and root exudates.

    Original languageEnglish
    Pages (from-to)763-766
    Number of pages4
    JournalJournal of Labelled Compounds and Radiopharmaceuticals
    Volume53
    Issue number13
    DOIs
    Publication statusPublished - 2010 Nov 1

    Keywords

    • multideuterated 5-deoxystrigol
    • strigolactone

    ASJC Scopus subject areas

    • Analytical Chemistry
    • Biochemistry
    • Radiology Nuclear Medicine and imaging
    • Drug Discovery
    • Spectroscopy
    • Organic Chemistry

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