Preparation of monodispersive fine particles of Pb(Zr 0.5Ti 0.5)O 3 from complex alkoxide

Tomoaki Satoh; Yosuke Yamamoto; Mikio Konno

Preparation of monodispersive fine particles of Pb(Zr _0.5Ti _0.5)O ₃ from complex alkoxide

Tomoaki Satoh, Yosuke Yamamoto, Mikio Konno

ENG - Chemical Engineering

Research output: Contribution to journal › Article › peer-review

Abstract

The sol-gel method is applied to the synthesis of Pb (Zr _0.5Ti _0.5) O ₃ particles with various post treatments. After the reaction of Pb(OAc) _z, Zr(OBu) ₄ and Ti(OEt) ₄ in ethanol solvent at 73°C over different reaction times, complex alkoxide is subjected to ammonia water and acetonitrile as a cosolvent at various water concentrations. The selection of reaction conditions enables the production of highly monodispersive particles with an average diameter less than 100 nm.

Original language	English
Number of pages	1
Journal	kagaku kogaku ronbunshu
Volume	23
Issue number	6
Publication status	Published - 1997 Dec 1

Keywords

Alkoxide
Chemical reaction
Ferroelectric material
Monodisperse particle
Powder

ASJC Scopus subject areas

Chemistry(all)
Chemical Engineering(all)

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title = "Preparation of monodispersive fine particles of Pb(Zr 0.5Ti 0.5)O 3 from complex alkoxide",

abstract = "The sol-gel method is applied to the synthesis of Pb (Zr 0.5Ti 0.5) O 3 particles with various post treatments. After the reaction of Pb(OAc) z, Zr(OBu) 4 and Ti(OEt) 4 in ethanol solvent at 73°C over different reaction times, complex alkoxide is subjected to ammonia water and acetonitrile as a cosolvent at various water concentrations. The selection of reaction conditions enables the production of highly monodispersive particles with an average diameter less than 100 nm.",

keywords = "Alkoxide, Chemical reaction, Ferroelectric material, Monodisperse particle, Powder",

author = "Tomoaki Satoh and Yosuke Yamamoto and Mikio Konno",

year = "1997",

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day = "1",

language = "English",

volume = "23",

journal = "Kagaku Kogaku Ronbunshu",

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TY - JOUR

T1 - Preparation of monodispersive fine particles of Pb(Zr 0.5Ti 0.5)O 3 from complex alkoxide

AU - Satoh, Tomoaki

AU - Yamamoto, Yosuke

AU - Konno, Mikio

PY - 1997/12/1

Y1 - 1997/12/1

N2 - The sol-gel method is applied to the synthesis of Pb (Zr 0.5Ti 0.5) O 3 particles with various post treatments. After the reaction of Pb(OAc) z, Zr(OBu) 4 and Ti(OEt) 4 in ethanol solvent at 73°C over different reaction times, complex alkoxide is subjected to ammonia water and acetonitrile as a cosolvent at various water concentrations. The selection of reaction conditions enables the production of highly monodispersive particles with an average diameter less than 100 nm.

AB - The sol-gel method is applied to the synthesis of Pb (Zr 0.5Ti 0.5) O 3 particles with various post treatments. After the reaction of Pb(OAc) z, Zr(OBu) 4 and Ti(OEt) 4 in ethanol solvent at 73°C over different reaction times, complex alkoxide is subjected to ammonia water and acetonitrile as a cosolvent at various water concentrations. The selection of reaction conditions enables the production of highly monodispersive particles with an average diameter less than 100 nm.

KW - Alkoxide

KW - Chemical reaction

KW - Ferroelectric material

KW - Monodisperse particle

KW - Powder

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M3 - Article

AN - SCOPUS:33751437557

VL - 23

JO - Kagaku Kogaku Ronbunshu

JF - Kagaku Kogaku Ronbunshu

SN - 0386-216X

IS - 6

ER -