Microreactor for synthesis via intermediates with assembled units enabling rapid mixing and heat transfer and short residence time

Nobuaki Aoki, Ryouhei Kitajima, Chiharu Itoh, Kazuhiro Mae

    Research output: Chapter in Book/Report/Conference proceedingConference contribution

    Abstract

    This paper describes a reactor for multi-step syntheses via intermediates with improved selectivity of desired products. This reactor is referred as assembled reactor. This reactor consists of mixing, residence time and heat exchange units. It was applied to the synthesis of bromobenzene via p-bromophenyllithium and gave the product yield > 80%. The assemble reactor enabled rapid mixing and heat transfer and short residence time between successive reaction steps and offers a opportunity to be used in multi-step syntheses via unstable intermediates with improved product distribution in industrial production. This is an abstract of a paper presented at the 42nd Loss Prevention Symposium (New Orleans, LA 4/6-10/2008).

    Original languageEnglish
    Title of host publication2008 AIChE Spring National Meeting, Conference Proceedings
    Publication statusPublished - 2008 Dec 23
    Event2008 AIChE Spring National Meeting, Conference - New Orleans, LA, United States
    Duration: 2008 Apr 62008 Apr 10

    Other

    Other2008 AIChE Spring National Meeting, Conference
    CountryUnited States
    CityNew Orleans, LA
    Period08/4/608/4/10

    Keywords

    • Assembled units
    • Heat transfer
    • Mixing
    • Residence Time
    • Synthesis via intermediates

    ASJC Scopus subject areas

    • Biotechnology
    • Chemical Engineering(all)
    • Bioengineering
    • Safety, Risk, Reliability and Quality

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