Abstract
This paper describes a reactor for multi-step syntheses via intermediates with improved selectivity of desired products. This reactor is referred as assembled reactor. This reactor consists of mixing, residence time and heat exchange units. It was applied to the synthesis of bromobenzene via p-bromophenyllithium and gave the product yield > 80%. The assemble reactor enabled rapid mixing and heat transfer and short residence time between successive reaction steps and offers a opportunity to be used in multi-step syntheses via unstable intermediates with improved product distribution in industrial production. This is an abstract of a paper presented at the 42nd Loss Prevention Symposium (New Orleans, LA 4/6-10/2008).
Original language | English |
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Title of host publication | 2008 AIChE Spring National Meeting, Conference Proceedings |
Publication status | Published - 2008 Dec 23 |
Event | 2008 AIChE Spring National Meeting, Conference - New Orleans, LA, United States Duration: 2008 Apr 6 → 2008 Apr 10 |
Other
Other | 2008 AIChE Spring National Meeting, Conference |
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Country | United States |
City | New Orleans, LA |
Period | 08/4/6 → 08/4/10 |
Keywords
- Assembled units
- Heat transfer
- Mixing
- Residence Time
- Synthesis via intermediates
ASJC Scopus subject areas
- Biotechnology
- Chemical Engineering(all)
- Bioengineering
- Safety, Risk, Reliability and Quality