Low-temperature synthesis of nanocrystalline ZrP via co-reduction of ZrCl4 and PCl3

Luyang Chen, Mingxing Huang, Yunle Gu, Liang Shi, Zeheng Yang, Yitai Qian

    Research output: Contribution to journalArticlepeer-review

    5 Citations (Scopus)

    Abstract

    Zirconium phosphide (ZrP) has been synthesized via a sodium co reduction of ZrCl4 and PCl3 at 350°C. The X-ray powder diffraction (XRD) pattern can be indexed as cubic ZrP with the lattice constant a=5.25 Å. The transmission electron microscopy (TEM) image indicates the product has dendritic morphology and hexagonal flakes.

    Original languageEnglish
    Pages (from-to)3337-3339
    Number of pages3
    JournalMaterials Letters
    Volume58
    Issue number26
    DOIs
    Publication statusPublished - 2004 Oct

    Keywords

    • Dendrites
    • Phosphides
    • X-ray diffraction

    ASJC Scopus subject areas

    • Materials Science(all)
    • Condensed Matter Physics
    • Mechanics of Materials
    • Mechanical Engineering

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