Low-temperature synthesis of nanocrystalline ZrB2 via co-reduction of ZrCl4 and BBr3

Luyang Chen, Yunle Gu, Liang Shi, Jianhua Ma, Zeheng Yang, Yitai Qian

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    2 Citations (Scopus)

    Abstract

    Nanocrystalline zirconium diboride (ZrB2) has been synthesized via a sodium co-reduction of ZrCl4 and BBr3 at 400 °C. The XRD patterns can be indexed as hexagonal ZrB2 with the lattice constants a = 3.167 and c = 3.527 Å. The TEM image indicates the product has particle morphology, with size of about 20 nm.

    Original languageEnglish
    Pages (from-to)1423-1424
    Number of pages2
    JournalBulletin of the Chemical Society of Japan
    Volume77
    Issue number7
    DOIs
    Publication statusPublished - 2004

    ASJC Scopus subject areas

    • Chemistry(all)

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