Low Temperature Synthesis and Characterization of Cubic CaB6 Ultrafine Powders

Liang Shi; Yunle Gu; Luyang Chen; Zeheng Yang; Jianhua Ma; Yitai Qian

doi:10.1246/cl.2003.958

Low Temperature Synthesis and Characterization of Cubic CaB₆ Ultrafine Powders

Liang Shi, Yunle Gu, Luyang Chen, Zeheng Yang, Jianhua Ma, Yitai Qian

Research output: Contribution to journal › Article

18 Citations (Scopus)

Abstract

Ultrafine calcium hexaboride (CaB₆) powder was successfully synthesized at 500°C in an autoclave by using CaCl₂ and NaBH ₄ as the reactants. X-ray powder diffraction pattern and Raman spectra indicate the formation of CaB₆. The atomic ratio of B to C of 5.91:1.0 was determined from X-ray photoelectron spectra.

Original language	English
Pages (from-to)	958-959
Number of pages	2
Journal	Chemistry Letters
Volume	32
Issue number	10
DOIs	https://doi.org/10.1246/cl.2003.958
Publication status	Published - 2003 Oct 5

ASJC Scopus subject areas

Chemistry(all)

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10.1246/cl.2003.958

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Shi, L., Gu, Y., Chen, L., Yang, Z., Ma, J., & Qian, Y. (2003). Low Temperature Synthesis and Characterization of Cubic CaB₆ Ultrafine Powders. Chemistry Letters, 32(10), 958-959. https://doi.org/10.1246/cl.2003.958

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abstract = "Ultrafine calcium hexaboride (CaB6) powder was successfully synthesized at 500°C in an autoclave by using CaCl2 and NaBH 4 as the reactants. X-ray powder diffraction pattern and Raman spectra indicate the formation of CaB6. The atomic ratio of B to C of 5.91:1.0 was determined from X-ray photoelectron spectra.",

author = "Liang Shi and Yunle Gu and Luyang Chen and Zeheng Yang and Jianhua Ma and Yitai Qian",

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AU - Shi, Liang

AU - Gu, Yunle

AU - Chen, Luyang

AU - Yang, Zeheng

AU - Ma, Jianhua

AU - Qian, Yitai

PY - 2003/10/5

Y1 - 2003/10/5

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AB - Ultrafine calcium hexaboride (CaB6) powder was successfully synthesized at 500°C in an autoclave by using CaCl2 and NaBH 4 as the reactants. X-ray powder diffraction pattern and Raman spectra indicate the formation of CaB6. The atomic ratio of B to C of 5.91:1.0 was determined from X-ray photoelectron spectra.

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