Environment-sensitive thermal coarsening of nanoporous gold

Satoko Kuwano-Nakatani, Takeshi Fujita, Kazuki Uchisawa, Daichi Umetsu, Yu Kase, Yusuke Kowata, Katsuhiko Chiba, Tomoharu Tokunaga, Shigeo Arai, Yuta Yamamoto, Nobuo Tanaka, Mingwei Chen

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13 Citations (Scopus)

Abstract

In order to investigate environmental effects on the ligament/pore coarsening of nanoporous gold (NPG), we studied the thermal coarsening of NPG both in air and vacuum by ex situ observation, and found that it has high structural stability against heat treatment in vacuum. To clarify the nature of this phenomenon, we investigated the thermal coarsening of NPG by in situ environmental transmission electron microscopy. At an elevated temperature (400°C), the coarsening of ligaments/pores was triggered by introducing either pure N2 or O2 gas into the transmission electron microscopy (TEM) chamber (but not by Ar gas). We thus conclude with a discussion on the mechanism for thermal coarsening of NPG.

Original languageEnglish
Pages (from-to)468-472
Number of pages5
JournalMaterials Transactions
Volume56
Issue number4
DOIs
Publication statusPublished - 2015

Keywords

  • Catalytic materials
  • Environmental factors
  • Environmental transmission electron microscopy
  • Nanoporous gold
  • Thermal coarsening

ASJC Scopus subject areas

  • Materials Science(all)
  • Condensed Matter Physics
  • Mechanics of Materials
  • Mechanical Engineering

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  • Cite this

    Kuwano-Nakatani, S., Fujita, T., Uchisawa, K., Umetsu, D., Kase, Y., Kowata, Y., Chiba, K., Tokunaga, T., Arai, S., Yamamoto, Y., Tanaka, N., & Chen, M. (2015). Environment-sensitive thermal coarsening of nanoporous gold. Materials Transactions, 56(4), 468-472. https://doi.org/10.2320/matertrans.MF201403