Comparison of ICP Atomic Emission Intensities on Axial and Radial Views, and Determination of Trace Amounts of As, Sb and Sn in Iron and Steel

Toshiko Itagaki; Kunio Takada; Kazuaki Wagatsuma; Kenji Abiko

doi:10.2355/tetsutohagane1955.89.9_890

Comparison of ICP Atomic Emission Intensities on Axial and Radial Views, and Determination of Trace Amounts of As, Sb and Sn in Iron and Steel

Toshiko Itagaki, Kunio Takada, Kazuaki Wagatsuma, Kenji Abiko

Materials Processing and Characterization Division

Research output: Contribution to journal › Article › peer-review

6 Citations (Scopus)

Abstract

Trace amounts of As, Sb and Sn in iron and steel were determined by ICP-OES. Intensities of some atomic emission lines were simultaneously determined from axial or radial view of argon plasma, Atomic emission intensities from the axial view were higher about 37 to 53 times than those from the radial view. Detection limits of As, Sb and Sn were order of 1 ppm in iron and steel by axial view measurement. Detection limit of As was lowered to order of 0.1 ppm after removal of iron as main component in sample solution with co-precipitation of MnO₂.

Original language	English
Pages (from-to)	890-894
Number of pages	5
Journal	Tetsu-To-Hagane/Journal of the Iron and Steel Institute of Japan
Volume	89
Issue number	9
DOIs	https://doi.org/10.2355/tetsutohagane1955.89.9_890
Publication status	Published - 2003 Sept

Keywords

Antimony
Arsenic
Axial view
Co-precipitation with manganese(IV) oxide
Inductively coupled plasma optical emission spectrometry (ICP-OES)
Iron
Radial view
Steel
Tin

ASJC Scopus subject areas

Condensed Matter Physics
Physical and Theoretical Chemistry
Metals and Alloys
Materials Chemistry

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10.2355/tetsutohagane1955.89.9_890

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Comparison of ICP Atomic Emission Intensities on Axial and Radial Views, and Determination of Trace Amounts of As, Sb and Sn in Iron and Steel. / Itagaki, Toshiko; Takada, Kunio; Wagatsuma, Kazuaki et al.

In: Tetsu-To-Hagane/Journal of the Iron and Steel Institute of Japan, Vol. 89, No. 9, 09.2003, p. 890-894.

Research output: Contribution to journal › Article › peer-review

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AU - Wagatsuma, Kazuaki

AU - Abiko, Kenji

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AB - Trace amounts of As, Sb and Sn in iron and steel were determined by ICP-OES. Intensities of some atomic emission lines were simultaneously determined from axial or radial view of argon plasma, Atomic emission intensities from the axial view were higher about 37 to 53 times than those from the radial view. Detection limits of As, Sb and Sn were order of 1 ppm in iron and steel by axial view measurement. Detection limit of As was lowered to order of 0.1 ppm after removal of iron as main component in sample solution with co-precipitation of MnO2.

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KW - Axial view

KW - Co-precipitation with manganese(IV) oxide

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Comparison of ICP Atomic Emission Intensities on Axial and Radial Views, and Determination of Trace Amounts of As, Sb and Sn in Iron and Steel

Abstract

Keywords

ASJC Scopus subject areas

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