Characterization of TiO2-Ag nanocomposite particles prepared by spray pyrolysis process using transmission electron microscopy and three-dimensional electron tomography

Kenji Kaneko; Won Jin Moon; Koji Inoke; Zenji Horita; Satoshi Ohara; Tadafumi Adschiri; Hiroya Abe; Makio Naito

doi:10.1016/j.msea.2005.05.056

Characterization of TiO₂-Ag nanocomposite particles prepared by spray pyrolysis process using transmission electron microscopy and three-dimensional electron tomography

Kenji Kaneko, Won Jin Moon, Koji Inoke, Zenji Horita, Satoshi Ohara, Tadafumi Adschiri, Hiroya Abe, Makio Naito

Advanced Institute for Materials Research (AIMR)

Research output: Contribution to journal › Article › peer-review

26 Citations (Scopus)

Abstract

TiO₂-Ag nanocomposite particles were prepared by spray pyrolysis of TiO₂ (7 nm) dispersed AgNO₃ solution. The structures and morphologies of powders were carefully characterized by combination of transmission electron microscopy (TEM) and three-dimensional electron tomography (3D-ET). It was clearly demonstrated by 3D-ET that the TiO₂-Ag nanocomposite particle was consisted of well-dispersed Ag nanoparticles within TiO₂ matrix. Furthermore, it was shown by high-resolution TEM that the spray pyrolysis was capable of fabricating Ag particles with a few nm in size.

Original language	English
Pages (from-to)	32-36
Number of pages	5
Journal	Materials Science and Engineering A
Volume	403
Issue number	1-2
DOIs	https://doi.org/10.1016/j.msea.2005.05.056
Publication status	Published - 2005 Aug 25

Keywords

Catalyst
Electron tomography
Nanocomposite
TEM
TiO

ASJC Scopus subject areas

Materials Science(all)
Condensed Matter Physics
Mechanics of Materials
Mechanical Engineering

Access to Document

10.1016/j.msea.2005.05.056

Cite this

Characterization of TiO₂-Ag nanocomposite particles prepared by spray pyrolysis process using transmission electron microscopy and three-dimensional electron tomography. / Kaneko, Kenji; Moon, Won Jin; Inoke, Koji et al.

In: Materials Science and Engineering A, Vol. 403, No. 1-2, 25.08.2005, p. 32-36.

Research output: Contribution to journal › Article › peer-review

Kaneko, K, Moon, WJ, Inoke, K, Horita, Z, Ohara, S, Adschiri, T, Abe, H & Naito, M 2005, 'Characterization of TiO₂-Ag nanocomposite particles prepared by spray pyrolysis process using transmission electron microscopy and three-dimensional electron tomography', Materials Science and Engineering A, vol. 403, no. 1-2, pp. 32-36. https://doi.org/10.1016/j.msea.2005.05.056

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abstract = "TiO2-Ag nanocomposite particles were prepared by spray pyrolysis of TiO2 (7 nm) dispersed AgNO3 solution. The structures and morphologies of powders were carefully characterized by combination of transmission electron microscopy (TEM) and three-dimensional electron tomography (3D-ET). It was clearly demonstrated by 3D-ET that the TiO2-Ag nanocomposite particle was consisted of well-dispersed Ag nanoparticles within TiO2 matrix. Furthermore, it was shown by high-resolution TEM that the spray pyrolysis was capable of fabricating Ag particles with a few nm in size.",

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AU - Ohara, Satoshi

AU - Adschiri, Tadafumi

AU - Abe, Hiroya

AU - Naito, Makio

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AB - TiO2-Ag nanocomposite particles were prepared by spray pyrolysis of TiO2 (7 nm) dispersed AgNO3 solution. The structures and morphologies of powders were carefully characterized by combination of transmission electron microscopy (TEM) and three-dimensional electron tomography (3D-ET). It was clearly demonstrated by 3D-ET that the TiO2-Ag nanocomposite particle was consisted of well-dispersed Ag nanoparticles within TiO2 matrix. Furthermore, it was shown by high-resolution TEM that the spray pyrolysis was capable of fabricating Ag particles with a few nm in size.

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