A method of determining residual monomer in acrylic resin using methyl ethyl ketone

Shinsuke Sadamori; Naofumi Shigeto; Taizo Hamada; Kyuichiro Okuda

doi:10.1111/j.1834-7819.1990.tb04681.x

A method of determining residual monomer in acrylic resin using methyl ethyl ketone

Shinsuke Sadamori, Naofumi Shigeto, Taizo Hamada, Kyuichiro Okuda

DEN - Dental Sciences

Research output: Contribution to journal › Article › peer-review

17 Citations (Scopus)

Abstract

An improved method of extraction of residual monomer from acrylic resin has been described for determination of the concentration of residual monomer by gas chromatography. Four kinds of organic solvent selected according to their physico‐chemical properties (methanol, N,N‐dimethylformamide, ethyl acetate and methyl ethyl ketone) were tested for their capacity to extract residual monomer at varying temperatures and time periods. Extraction with methyl ethyl ketone at 4°C was found to be the most effective. The method is simpler and more effective than others reported so far, and therefore seems to be suitable for clinical laboratory use. 1990 Australian Dental Association

Original language	English
Pages (from-to)	509-513
Number of pages	5
Journal	Australian Dental Journal
Volume	35
Issue number	6
DOIs	https://doi.org/10.1111/j.1834-7819.1990.tb04681.x
Publication status	Published - 1990 Jan 1

Keywords

Acrylic resin
methyl ethyl ketone
residual monomer

ASJC Scopus subject areas

Dentistry(all)

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N2 - An improved method of extraction of residual monomer from acrylic resin has been described for determination of the concentration of residual monomer by gas chromatography. Four kinds of organic solvent selected according to their physico‐chemical properties (methanol, N,N‐dimethylformamide, ethyl acetate and methyl ethyl ketone) were tested for their capacity to extract residual monomer at varying temperatures and time periods. Extraction with methyl ethyl ketone at 4°C was found to be the most effective. The method is simpler and more effective than others reported so far, and therefore seems to be suitable for clinical laboratory use. 1990 Australian Dental Association

AB - An improved method of extraction of residual monomer from acrylic resin has been described for determination of the concentration of residual monomer by gas chromatography. Four kinds of organic solvent selected according to their physico‐chemical properties (methanol, N,N‐dimethylformamide, ethyl acetate and methyl ethyl ketone) were tested for their capacity to extract residual monomer at varying temperatures and time periods. Extraction with methyl ethyl ketone at 4°C was found to be the most effective. The method is simpler and more effective than others reported so far, and therefore seems to be suitable for clinical laboratory use. 1990 Australian Dental Association

KW - Acrylic resin

KW - methyl ethyl ketone

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