A highly sensitive fluorescence method reveals the presence of palladium in a cross-coupling reaction mixture not treated with transition metals

Kiyofumi Inamoto, Laura D. Campbell, Takayuki Doi, Kazunori Koide

Research output: Contribution to journalArticle

24 Citations (Scopus)

Abstract

We previously reported a Suzuki-Miyaura coupling in dimethyl carbonate without adding additional transition metals. Here, we show an analysis of the reaction mixture that revealed the presence of palladium using a fluorogenic Tsuji-Trost reaction.

Original languageEnglish
Pages (from-to)3147-3148
Number of pages2
JournalTetrahedron Letters
Volume53
Issue number25
DOIs
Publication statusPublished - 2012 Jun 20

Keywords

  • Catalysis
  • Fluorescence spectroscopy
  • Palladium
  • Sensor
  • Suzuki-Miyaura coupling

ASJC Scopus subject areas

  • Biochemistry
  • Drug Discovery
  • Organic Chemistry

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