A facile route to VN and V2O3 nanocrystals from single precursor NH4VO3

Zeheng Yang, Peijun Cai, Luyang Chen, Yunle Gu, Liang Shi, Aiwu Zhao, Yitai Qian

    Research output: Contribution to journalArticle

    21 Citations (Scopus)

    Abstract

    V2O3 and VN nanocrystals have been synthesized by the decomposition of the precursor NH4VO3 and following nitridation in an autoclave with metallic Na flux at 450-600 °C. X-ray powder diffraction (XRD) recorded the evolution process of the reaction from precursor NH4VO3 to hexagonal V2O3 and then to NaCl-type VN. In addition, the products were characterized by X-ray photoelectron spectroscopy (XPS) and transmission electron microscopy (TEM).

    Original languageEnglish
    Pages (from-to)229-232
    Number of pages4
    JournalJournal of Alloys and Compounds
    Volume420
    Issue number1-2
    DOIs
    Publication statusPublished - 2006 Aug 31

    Keywords

    • Chemical synthesis
    • Nanostructure
    • Transmission electron microscopy
    • X-ray diffraction

    ASJC Scopus subject areas

    • Mechanics of Materials
    • Mechanical Engineering
    • Metals and Alloys
    • Materials Chemistry

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  • Cite this

    Yang, Z., Cai, P., Chen, L., Gu, Y., Shi, L., Zhao, A., & Qian, Y. (2006). A facile route to VN and V2O3 nanocrystals from single precursor NH4VO3. Journal of Alloys and Compounds, 420(1-2), 229-232. https://doi.org/10.1016/j.jallcom.2005.08.085