A facile chromatographic method for purification of pinacol boronic esters

Shunpei Hitosugi; Daiki Tanimoto; Waka Nakanishi; Hiroyuki Isobe

doi:10.1246/cl.2012.972

A facile chromatographic method for purification of pinacol boronic esters

Shunpei Hitosugi, Daiki Tanimoto, Waka Nakanishi, Hiroyuki Isobe

SCI - Chemistry

Research output: Contribution to journal › Article › peer-review

27 Citations (Scopus)

Abstract

A facile chromatographic method for purification of pinacol boronic esters has been developed. Impregnation of silica gel with boric acid was effective both for thin layer chromatography (TLC) and for flash column chromatography. Purification of a series of pinacol boronic esters was successful by suppressing loss of the compounds due to over-adsorption.

Original language	English
Pages (from-to)	972-973
Number of pages	2
Journal	Chemistry Letters
Volume	41
Issue number	9
DOIs	https://doi.org/10.1246/cl.2012.972
Publication status	Published - 2012

ASJC Scopus subject areas

Chemistry(all)

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10.1246/cl.2012.972

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abstract = "A facile chromatographic method for purification of pinacol boronic esters has been developed. Impregnation of silica gel with boric acid was effective both for thin layer chromatography (TLC) and for flash column chromatography. Purification of a series of pinacol boronic esters was successful by suppressing loss of the compounds due to over-adsorption.",

author = "Shunpei Hitosugi and Daiki Tanimoto and Waka Nakanishi and Hiroyuki Isobe",

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AU - Tanimoto, Daiki

AU - Nakanishi, Waka

AU - Isobe, Hiroyuki

PY - 2012

Y1 - 2012

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AB - A facile chromatographic method for purification of pinacol boronic esters has been developed. Impregnation of silica gel with boric acid was effective both for thin layer chromatography (TLC) and for flash column chromatography. Purification of a series of pinacol boronic esters was successful by suppressing loss of the compounds due to over-adsorption.

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JO - Chemistry Letters

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A facile chromatographic method for purification of pinacol boronic esters

Abstract

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