A convenient solid-state reaction route to nanocrystalline TiB2

Liang Shi; Yunle Gu; Luyang Chen; Zeheng Yang; Jianhua Ma; Yitai Qian

doi:10.1016/j.inoche.2003.11.005

A convenient solid-state reaction route to nanocrystalline TiB₂

Liang Shi, Yunle Gu, Luyang Chen, Zeheng Yang, Jianhua Ma, Yitai Qian

Research output: Contribution to journal › Article › peer-review

17 Citations (Scopus)

Abstract

Nanocrystalline titanium diboride (TiB₂) powders were successfully synthesized at 650°C by using TiCl₄, Mg and MgB ₂ as the reactants. Transmission electron microscopy images show that typical TiB₂ crystallites are composed of uniform particles with the average grain size of about 40 nm.

Original language	English
Pages (from-to)	192-194
Number of pages	3
Journal	Inorganic Chemistry Communications
Volume	7
Issue number	2
DOIs	https://doi.org/10.1016/j.inoche.2003.11.005
Publication status	Published - 2004 Feb

Keywords

Chemical synthesis
Nanocrystals
Titanium diboride
X-ray powder diffraction

ASJC Scopus subject areas

Physical and Theoretical Chemistry
Inorganic Chemistry
Materials Chemistry

Access to Document

10.1016/j.inoche.2003.11.005

Cite this

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title = "A convenient solid-state reaction route to nanocrystalline TiB2",

abstract = "Nanocrystalline titanium diboride (TiB2) powders were successfully synthesized at 650°C by using TiCl4, Mg and MgB 2 as the reactants. Transmission electron microscopy images show that typical TiB2 crystallites are composed of uniform particles with the average grain size of about 40 nm.",

keywords = "Chemical synthesis, Nanocrystals, Titanium diboride, X-ray powder diffraction",

author = "Liang Shi and Yunle Gu and Luyang Chen and Zeheng Yang and Jianhua Ma and Yitai Qian",

year = "2004",

month = feb,

doi = "10.1016/j.inoche.2003.11.005",

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AU - Shi, Liang

AU - Gu, Yunle

AU - Chen, Luyang

AU - Yang, Zeheng

AU - Ma, Jianhua

AU - Qian, Yitai

PY - 2004/2

Y1 - 2004/2

N2 - Nanocrystalline titanium diboride (TiB2) powders were successfully synthesized at 650°C by using TiCl4, Mg and MgB 2 as the reactants. Transmission electron microscopy images show that typical TiB2 crystallites are composed of uniform particles with the average grain size of about 40 nm.

AB - Nanocrystalline titanium diboride (TiB2) powders were successfully synthesized at 650°C by using TiCl4, Mg and MgB 2 as the reactants. Transmission electron microscopy images show that typical TiB2 crystallites are composed of uniform particles with the average grain size of about 40 nm.

KW - Chemical synthesis

KW - Nanocrystals

KW - Titanium diboride

KW - X-ray powder diffraction

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