A convenient new route from diphosphene to 1,3-diphospha-allene and dynamic NMR studies of the 2,4,6-tri-t-butylphenyl derivative

Masaaki Yoshifuji; Shigeru Sasaki; Takashi Niitsu; Naoki Inamoto

doi:10.1016/S0040-4039(00)95155-4

A convenient new route from diphosphene to 1,3-diphospha-allene and dynamic NMR studies of the 2,4,6-tri-t-butylphenyl derivative

Masaaki Yoshifuji, Shigeru Sasaki, Takashi Niitsu, Naoki Inamoto

Research output: Contribution to journal › Article › peer-review

43 Citations (Scopus)

Abstract

Addition of dihalocarbenes to a diphosphene gave diphosphiranes which undergo rearrangement on treatment with alkyllithium reagents to afford 1,3-diphospha-allene; dynamic NMR studies on the allene are described.

Original language	English
Pages (from-to)	187-188
Number of pages	2
Journal	Tetrahedron Letters
Volume	30
Issue number	2
DOIs	https://doi.org/10.1016/S0040-4039(00)95155-4
Publication status	Published - 1989 Jan 1
Externally published	Yes

ASJC Scopus subject areas

Biochemistry
Drug Discovery
Organic Chemistry

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abstract = "Addition of dihalocarbenes to a diphosphene gave diphosphiranes which undergo rearrangement on treatment with alkyllithium reagents to afford 1,3-diphospha-allene; dynamic NMR studies on the allene are described.",

author = "Masaaki Yoshifuji and Shigeru Sasaki and Takashi Niitsu and Naoki Inamoto",

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AU - Sasaki, Shigeru

AU - Niitsu, Takashi

AU - Inamoto, Naoki

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AB - Addition of dihalocarbenes to a diphosphene gave diphosphiranes which undergo rearrangement on treatment with alkyllithium reagents to afford 1,3-diphospha-allene; dynamic NMR studies on the allene are described.

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