3D morphological evolution of porous titanium by x-ray micro- and nano-tomography

Yu Chen Karen Chen-Wiegart, Takeshi Wada, Nikita Butakov, Xianghui Xiao, Francesco De Carlo, Hidemi Kato, Jun Wang, David C. Dunand, Eric Maire

Research output: Contribution to journalArticle

27 Citations (Scopus)

Abstract

The 3D morphological evolution of titanium foams as they undergo a two-step fabrication process is quantitatively characterized through x-ray micro- and nano-tomography. In the first process step, a Cu-Ti-Cr-Zr prealloy is immersed in liquid Mg, where Cu is alloyed with Mg while a skeleton of crystalline Ti-Cr-Zr is created. In the second step, the Mg-Cu phase is etched in acid, leaving a Ti-Cr-Zr foam with submicron struts. 3D images of these solidified Ti-Cr-Zr/Mg-Cu composites and leached Ti-Cr-Zr foams are acquired after 5, 10, and 30 min exposure to liquid Mg. As the Mg exposure time increases, the Ti-Cr-Zr ligaments grow in size. The tortuosity loosely follows the Bruggeman relation. The interfacial surface distribution of these Ti-foams is qualitatively similar to other nano-porous metal prepared by one-step dealloying. The characteristic length of the Mg-Cu phase and pores are also reported.

Original languageEnglish
Pages (from-to)2444-2452
Number of pages9
JournalJournal of Materials Research
Volume28
Issue number17
DOIs
Publication statusPublished - 2013 Sep 14

ASJC Scopus subject areas

  • Materials Science(all)
  • Condensed Matter Physics
  • Mechanics of Materials
  • Mechanical Engineering

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    Chen-Wiegart, Y. C. K., Wada, T., Butakov, N., Xiao, X., De Carlo, F., Kato, H., Wang, J., Dunand, D. C., & Maire, E. (2013). 3D morphological evolution of porous titanium by x-ray micro- and nano-tomography. Journal of Materials Research, 28(17), 2444-2452. https://doi.org/10.1557/jmr.2013.151