3D image analysis of Pd particles formed on porous polymeric support

Yukihiro Nishikawa, Takeshi Kaneko, Kaoru Yasuda, Toshio Nishi, Hirokazu Hasegawa, Hiroshi Jinnai

Research output: Contribution to conferencePaper

Abstract

Size and position of metal particles on porous polymeric support were studied by transmission electron microtomography (TEMT). The porous polymeric support was prepared by ozonolysis of the polyisoprene microdomains of gyroid microphase-separated structure consisting of poly(2-vinylpryridine-block- isoprene), Then palladium metal particles were formed by reduction of Pd ions in toluene/1-propanol solvent. Pd particles on the polymer support were clearly visualized by TEMT. The size and spatial distribution of Pd particles were analyzed by 3D image analysis. Furthermore, the spatial density of Pd particles was also determined with respect to not only volume but also the surface area of the polymer support.

Original languageEnglish
Number of pages1
Publication statusPublished - 2005 Dec 1
Externally publishedYes
Event54th SPSJ Annual Meeting 2005 - Yokohama, Japan
Duration: 2005 May 252005 May 27

Other

Other54th SPSJ Annual Meeting 2005
CountryJapan
CityYokohama
Period05/5/2505/5/27

Keywords

  • 3D image analysis
  • Block copolymer
  • Gyroid structure
  • Nano particle
  • Transmission Electron Microtomography

ASJC Scopus subject areas

  • Engineering(all)

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  • Cite this

    Nishikawa, Y., Kaneko, T., Yasuda, K., Nishi, T., Hasegawa, H., & Jinnai, H. (2005). 3D image analysis of Pd particles formed on porous polymeric support. Paper presented at 54th SPSJ Annual Meeting 2005, Yokohama, Japan.